Recieved:

13/07/2019

Accepted:

16/09/2019

Page: 

167

182

doi:

http://dx.doi.org/10.17515/resm2019.139ma0713

Views:

3173
Cited 10 times

Preparation and characterization of a new adsorbent from raphia taedigera seed

Emmanuel Folorunso Olasehinde1, Segun Michael Abegunde2

1Department of Chemistry, Federal University of Technology, Akure, Nigeria
2Department of Science Technology, Federal Polytechnic, Ado-Ekiti, Ekiti State, Nigeria

Abstract

There has been widespread research and engagement in recent years on the use of plant material in preparing porous carbon for wastewater treatment. In this study, new biochars (BCs) impregnated with 0.1 M sulphuric acid (RTA) and 0.1 M sodium hydroxide (RTB) were prepared. The BCs and raw seed [RTR] were characterized using scanning electron microscopy (SEM), Fourier-transform infrared (FTIR) spectrophotometer, and thermogravimetric/Differential thermal analyser. [TGA/DTA) to determine their morphology, spectral bands and thermal behaviour respectively. RTR showed a scattered aggregated surface microstructure, while both RTA and RTB gave aggregated rough surfaces with high number of pores. The FTIR analysis showed significant changes in term of band shift, bands disappearances, and new band formations due to pyrolysis and activation of the BCs. The results of the TGA/DTA revealed that RTA and RTB have better thermal stability than RTR, with the maximum degradation temperature of RTR, RTA, and RTB occurred at 3800C, 4250C and 4100C respectively. Adsorption efficiencies ranged from 81.671 to 99.743% for performance evaluation on the BCs using different adsorbent dosages and the initial concentrations of methylene blue solutions. These preliminary investigations suggest that biochars synthesized from Raphia taedigera seed can be used for methylene blue removal from wastewater.

Keywords

Raphia taedigera; adsorbent; carbonization; activation; methylene blue; SEM
Cited 7 times in the last 5 years and 10 times in total in articles indexed in Scopus.

Cite this article as: 

Olasehinde EF, Abegunde SM. Preparation and characterization of a new adsorbent from raphia taedigera seed. Res. Eng. Struct. Mater., 2020; 6(2): 167-182.
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